紫芝超细粉挥发油成分GC-MS分析 |
GC-MS analysis of chemical components in the essential oils of from the ultrafine-powder of Ganoderma sinense |
投稿时间:2006-07-30 修订日期:2006-09-10 |
中文关键词:紫芝,超细粉,挥发油,化学成分 |
英文关键词:Ganoderma sinense, ultra-fine powder, esstional oil, chemical component |
基金项目:福建省自然科学基金计划项目(No.C9810041);福建省科技计划重点项目(No.2007I0103) |
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中文摘要: |
将紫芝Ganoderma sinense(“闽紫96”,HMAS 77207,阔叶树枝桠材或边材栽培)超微粉碎加工成500目的子实体超细粉。激光粒度分析表明:紫芝超细粉的表面积到834.18m2/kg,中位径(D50)为12.68μm。气质联用分析结果表明:从紫芝超细粉挥发油中分离到35种成分,出峰时间为7.872~30.239min,确定了其中32个成分,占相对含量的88.642%;绝大多数成分为脂肪族化合物(67.216%),主要成分(20.67%)为2,6-二叔丁基-苯酚为芳香族化合物,还检出2种杂环族化合物。 |
英文摘要: |
The fruitbodies of Ganoderma sinense (“Minzi 96” strain, HAMS 77207, cultivated with laburnum or branches of broadleaf tree) were processed into ultrafine-powder that sifted through Φ500 R40/3 sieve. And the granularity were tested by laser grain-size analysis, that specific surface area (BET)was 834.18m2/kg, and the cumulative distribution data D50 was 12.68μm(equivalent grain-size). 35 compositions of total essential oil from the ultrafine-powder were separated and identified by GC-MS, retention time arranged from 7.872 min to 30.239min. The results indicated that 32 compounds were determinated, and their relative contents were about 88.64%, most of the compounds belong to aliphatic compounds (67.216%), and the main constituent with highest relative content (20.67%) have been identified as 2,6-di-tert-butylphenol(aromatics compounds), moreover, two compounds of heterocyclics were also checked out. |
陈体强,吴锦忠,朱金荣. 紫芝超细粉挥发油成分GC-MS分析[J]. 菌物学报, 2007, 26(2): 279-283 |
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